Hydrazine → HCID 18356908, compound

HRID 427257Notes

Reaction equation

HRID 427257 reaction equation
[N+:1]([C:4]1[N:5]=[CH:6][N:7]([CH2:9][CH2:10][CH2:11][CH2:12][N:13]2C(=O)C3C(=CC=CC=3)C2=O)[CH:8]=1)([O-:3])=[O:2].NN>C(O)C>[N+:1]([C:4]1[N:5]=[CH:6][N:7]([CH2:9][CH2:10][CH2:11][CH2:12][NH2:13])[CH:8]=1)([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 18356907HCID 18356907, compound

Product 1

HCID 18356908HCID 18356908, compoundYield 169.2%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A mixture of 33.31 g of the product of Stage A, 555 ml of ethanol and 11.33 ml of hydrazine are taken to reflux for 20 hours. After filtering, the reaction medium is left to return to ambient temperature and brought to dryness. 33.04 g of product is obtained.

Workup

  1. temperatureto reflux for 20 hours
  2. filtrationAfter filtering
  3. waitthe reaction medium is left
  4. customto return to ambient temperature

Sources & evidence

ORD record
ord-90575a5d6e364a2193aac03df64e5d57
Source dataset
uspto-grants-2001_11
Patent number
US06313101B1

Reaction notes

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