HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 2724874, compound → HCID 69557076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 2724874 | HCID 2724874 | — |
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Product | HCID 69557076 | HCID 69557076 | 97.5% |
Reaction Steps
To 1N HCl/MeOH (50 mL) at 0° C. was added (S)-2-Amino-3-benzylamino-propanoic acid (0.5 g, 2.57 mmol). Reaction was stirred at room temperature overnight. Volatiles were removed to give the product 2-Amino-3-benzylamino-propanoic acid methyl ester dihydrochloride salt as a white solid (0.7 g, 97.5%). MS: m/z=209 M+1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313117B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-0bf51751d7704ef6829f568b2f139c53 |
| Source note | uspto-grants-2001_11 |