HCID 18357125, compound → HCID 54566673, compound
Reaction equation
[N:1]1[CH:6]=[CH:5][C:4]([N:7]2[CH2:11][CH2:10][CH:9]([O:12][C:13]3[CH:18]=[CH:17][C:16](SCC4C=CC(OC)=CC=4)=[CH:15][N:14]=3)[CH2:8]2)=[CH:3][CH:2]=1.[NH4+].[OH-].C(Cl)Cl>>[N:1]1[CH:2]=[CH:3][C:4]([N:7]2[CH2:11][CH2:10][C@@H:9]([O:12][C:13]3[CH:18]=[CH:17][C:16]4[C:15](=[CH:2][CH:3]=[CH:4][CH:5]=4)[N:14]=3)[CH2:8]2)=[CH:5][CH:6]=1Participants
3
Procedure
Rf=0.37 (10%MeOH/1%NH4OH/CH2Cl2)
Sources & evidence
- ORD record
- ord-b5a51a85e3c442edb10d09d87ea8b031
- Source dataset
- uspto-grants-2001_11
- Patent number
- US06313127B1
Reaction notes
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