Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Ethylbenzoyl chloride → n1-(4-Methoxybenzoyl)-n2-(4-ethylbenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Ethylbenzoyl chloride | HCID 85368 | — |
| 반응물 | N1-(4-methoxybenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine | HCID 54024338 | — |
| 생성물 | n1-(4-Methoxybenzoyl)-n2-(4-ethylbenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine | HCID 10577465 | 88.1% |
반응 단계
Using the procedure described in Example 68, Part A, N1-(4-methoxybenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine (300 mg, 0.81 mmol) was reacted with 4-ethylbenzoyl chloride (0.13 mL, 0.89 mmol) to yield 360 mg (88%) of the title compound as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06313122B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-64c1304051814ab2b33d01f93d4d5d48 |
| 출처 메모 | uspto-grants-2001_11 |