4-Methoxy-2-nitroaniline → HCID 4598169, compound

HRID 427593Notes

Reaction equation

HRID 427593 reaction equation
[CH3:1][O:2][C:3]1[CH:9]=[CH:8][C:6]([NH2:7])=[C:5]([N+:10]([O-:12])=[O:11])[CH:4]=1.[C:13]([C:17]1[CH:25]=[CH:24][C:20]([C:21](Cl)=[O:22])=[CH:19][CH:18]=1)([CH3:16])([CH3:15])[CH3:14]>>[CH3:1][O:2][C:3]1[CH:9]=[CH:8][C:6]([NH:7][C:21](=[O:22])[C:20]2[CH:24]=[CH:25][C:17]([C:13]([CH3:15])([CH3:14])[CH3:16])=[CH:18][CH:19]=2)=[C:5]([N+:10]([O-:12])=[O:11])[CH:4]=1

Participants

3

Reactant 2

HCID 667934-Methoxy-2-nitroanilineHCID 743724-tert-Butylbenzoyl chloride

Product 1

HCID 4598169HCID 4598169, compoundYield 100%

Procedure

Using the procedure described in Example 68, Part A, 4-methoxy-2-nitroaniline (1.0 g, 3.4 mmol) was reacted with 4-tert-butylbenzoyl chloride to yield 1.45 g (100%) of the title compound as a yellow solid.

Sources & evidence

ORD record
ord-38e4db3366fd4f9da9947ff9b2538b5d
Source dataset
uspto-grants-2001_11
Patent number
US06313122B1

Reaction notes

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