2-Nitrobenzoyl chloride → HCID 18174420, compound

HRID 427605Notes

Reaction equation

HRID 427605 reaction equation
[N+:1]([C:4]1[CH:12]=[CH:11][CH:10]=[CH:9][C:5]=1[C:6](Cl)=[O:7])([O-:3])=[O:2].[NH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[C:16]([N:20]2[C:24](=[O:25])[C:23]3=[CH:26][CH:27]=[CH:28][CH:29]=[C:22]3[C:21]2=[O:30])[N:15]=1>>[C:21]1(=[O:30])[N:20]([C:16]2[N:15]=[C:14]([NH:13][C:6](=[O:7])[C:5]3[CH:9]=[CH:10][CH:11]=[CH:12][C:4]=3[N+:1]([O-:3])=[O:2])[CH:19]=[CH:18][CH:17]=2)[C:24](=[O:25])[C:23]2=[CH:26][CH:27]=[CH:28][CH:29]=[C:22]12

Participants

3

Reactant 2

HCID 118752-Nitrobenzoyl chlorideHCID 2731643HCID 2731643, compound

Product 1

HCID 18174420HCID 18174420, compoundYield 80.2%

Procedure

Using the procedure described in Example 93, Part A, 2-nitrobenzoyl chloride (2.3 mmol) and 2-amino-6-phthalimidopyridine (2.1 mmol) yielded 654 mg (80%) of the title compound.

Sources & evidence

ORD record
ord-825cb053f1ed4c9b90371703b1e9d024
Source dataset
uspto-grants-2001_11
Patent number
US06313122B1

Reaction notes

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