2-Nitroaniline → HCID 5161241, compound

HRID 427619Notes

Reaction equation

HRID 427619 reaction equation
[C:1]([C:5]1[CH:13]=[CH:12][C:8]([C:9](Cl)=[O:10])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[N+:14]([C:17]1[CH:23]=[CH:22][CH:21]=[CH:20][C:18]=1[NH2:19])([O-:16])=[O:15]>>[N+:14]([C:17]1[CH:23]=[CH:22][CH:21]=[CH:20][C:18]=1[NH:19][C:9](=[O:10])[C:8]1[CH:12]=[CH:13][C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])=[CH:6][CH:7]=1)([O-:16])=[O:15]

Participants

3

Reactant 2

HCID 69462-NitroanilineHCID 743724-tert-Butylbenzoyl chloride

Product 1

HCID 5161241HCID 5161241, compoundYield 100%

Procedure

Using the procedure described in Example 93, Part A, 4-tert-butylbenzoyl chloride (398 mmol) and 2-nitroaniline (362 mmol) yielded 21.6 g (100%) of the title compound.

Sources & evidence

ORD record
ord-3b6d75fbd1674ca190b8a855b3eae9dc
Source dataset
uspto-grants-2001_11
Patent number
US06313122B1

Reaction notes

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