Benzoyl chloride, 3-nitro- → HCID 31974248, compound

HRID 427625Notes

Reaction equation

HRID 427625 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7](Cl)=[O:8])([O-:3])=[O:2].[C:13]([C:17]1[CH:32]=[CH:31][C:20]([C:21]([NH:23][C:24]2[C:25]([NH2:30])=[CH:26][CH:27]=[CH:28][CH:29]=2)=[O:22])=[CH:19][CH:18]=1)([CH3:16])([CH3:15])[CH3:14]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7]([NH:30][C:25]1[C:24]([NH:23][C:21](=[O:22])[C:20]2[CH:31]=[CH:32][C:17]([C:13]([CH3:15])([CH3:14])[CH3:16])=[CH:18][CH:19]=2)=[CH:29][CH:28]=[CH:27][CH:26]=1)=[O:8])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 8495Benzoyl chloride, 3-nitro-HCID 1133079N-(2-aminophenyl)-4-tert-butylbenzamide

Product 1

HCID 31974248HCID 31974248, compoundYield 56.8%

Procedure

Using the procedure described in Example 93, Part A, 3-nitrobenzoyl chloride (2.2 mmol) and N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (1.8 mmol) yielded 427 mg (56%) of the title compound.

Sources & evidence

ORD record
ord-a6a303ee441d4ac98ad1d82dfd93552c
Source dataset
uspto-grants-2001_11
Patent number
US06313122B1

Reaction notes

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