p-Anisoyl chloride → 3,6-Dimethoxy-N1,N2-bis(4-methoxybenzoyl)-1,2-benzenediamine

HRID 427628Notes

Reaction equation

HRID 427628 reaction equation
[C:1](Cl)(=[O:10])[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=1.[CH3:12][O:13][C:14]1[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[C:16]([NH2:22])[C:15]=1[NH2:23]>>[CH3:21][O:20][C:17]1[CH:18]=[CH:19][C:14]([O:13][CH3:12])=[C:15]([NH:23][C:1](=[O:10])[C:2]2[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=2)[C:16]=1[NH:22][C:1](=[O:10])[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 116296603,6-Dimethoxybenzene-1,2-diamine

Product 1

HCID 105990433,6-Dimethoxy-N1,N2-bis(4-methoxybenzoyl)-1,2-benzenediamineYield 65%

Procedure

Using the procedure described in Example 93, Part A, 4-anisoyl chloride (4.9 mmol) and 3,6-dimethoxy-1,2-benzenediamine (2.0 mmol) yielded 555 mg (65%) of the title compound.

Sources & evidence

ORD record
ord-42aad58a5b4842ddaccda0bdbfe8c8bb
Source dataset
uspto-grants-2001_11
Patent number
US06313122B1

Reaction notes

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