4-Bromoaniline → N-(4-bromophenyl)-2-nitrobenzamide

HRID 427686Notes

Reaction equation

HRID 427686 reaction equation
[Br:1][C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.[N+:9]([C:12]1[CH:20]=[CH:19][CH:18]=[CH:17][C:13]=1[C:14](Cl)=[O:15])([O-:11])=[O:10]>>[N+:9]([C:12]1[CH:20]=[CH:19][CH:18]=[CH:17][C:13]=1[C:14]([NH:6][C:5]1[CH:7]=[CH:8][C:2]([Br:1])=[CH:3][CH:4]=1)=[O:15])([O-:11])=[O:10]

Participants

3

Reactant 2

HCID 78074-BromoanilineHCID 118752-Nitrobenzoyl chloride

Product 1

HCID 695259N-(4-bromophenyl)-2-nitrobenzamideYield 93%

Procedure

Using the procedure described in Example 93, Part A, 4-bromoaniline (11.6 mmol) and 2-nitrobenzoyl chloride (12.8 mmol) yielded 3.46 g (93%) of the title compound.

Sources & evidence

ORD record
ord-1271b06c4aae4aa4bc739d8fa6f748d7
Source dataset
uspto-grants-2001_11
Patent number
US06313122B1

Reaction notes

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