p-Anisoyl chloride → HCID 15908564, compound

HRID 428019Notes

Reaction equation

HRID 428019 reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](Cl)=[O:8])=[CH:5][CH:4]=1.[N:12]1[CH:17]=[CH:16][C:15]([C:18]2[CH:33]=[CH:32][C:21]([C:22]([NH:24][C:25]3[CH:26]=[N:27][CH:28]=[CH:29][C:30]=3[NH2:31])=[O:23])=[CH:20][CH:19]=2)=[CH:14][CH:13]=1>>[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([NH:31][C:30]2[CH:29]=[CH:28][N:27]=[CH:26][C:25]=2[NH:24][C:22](=[O:23])[C:21]2[CH:20]=[CH:19][C:18]([C:15]3[CH:14]=[CH:13][N:12]=[CH:17][CH:16]=3)=[CH:33][CH:32]=2)=[O:8])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 12069545HCID 12069545, compound

Product 1

HCID 15908564HCID 15908564, compoundYield 4%

Procedure

Using 4-methoxybenzoyl chloride and a similar procedure to that described for Example 2, Part C, N3-[4-(4-pyridyl)-benzoyl]-3,4-pyridinediamine (55 mg, 0.19 mmol) yielded 3.2 mg (4%) of the title compound.

Sources & evidence

ORD record
ord-c36ed5a4bd904bad9b609042e7082f97
Source dataset
uspto-grants-2001_11
Patent number
US06313151B1

Reaction notes

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