HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)benzeneacetic acid → 2-[(3-trifluoromethylphenyl)acetamido]butyric Acid Iso-butyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)benzeneacetic acid | HCID 67695 | — |
| Reactant | Isobutyl 2-aminobutyrate | HCID 13743360 | — |
| Product | 2-[(3-trifluoromethylphenyl)acetamido]butyric Acid Iso-butyl Ester | HCID 15481772 | — |
Reaction Steps
Following General Procedure I above and using 3-trifluoromethyl-phenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure J above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313152B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-03085cae310542718f0793f462b92fe1 |
| Source note | uspto-grants-2001_11 |