HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylcyclopentanol → N-[(3-chlorophenyl)acetyl]aianine 2-methylcyclopentyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylcyclopentanol | HCID 32205 | — |
| Reactant | N-(3-chlorophenylacetyl)alanine | HCID 15481783 | — |
| Product | N-[(3-chlorophenyl)acetyl]aianine 2-methylcyclopentyl Ester | HCID 54518082 | — |
Reaction Steps
Following General Procedure C above, and using N-(3-chlorophenylacetyl alanine (from Example D above) and 2-methylcyclopentanol (Aldrich) the title compound can be prepared. The reaction was monitored by tlc on silica gel and purification was by liquid chromatography using 3:7 EtOAc:hexane as the eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313152B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-d17f46fdca7e4c38bdbb6dec8bd36805 |
| Source note | uspto-grants-2001_11 |