HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 18177412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 18177431 | HCID 18177431 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18177412 | HCID 18177412 | — |
Reaction Steps
0.34 g (1.38 mmol) of the amine obtained in Step F is acetylated with acetic anhydride in pyridine according to the usual procedure. The crude product of that reaction is purified on a silica column (eluant:ethyl acetate) to yield the title acetamide in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313160B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-e34716af9be04819945c01236e1124f7 |
| Source note | uspto-grants-2001_11 |