HCID 136364246, compound → HCID 54145726, compound

HRID 428335Notes

Reaction equation

HRID 428335 reaction equation
[CH:1]([N:4]([CH:32]([CH3:34])[CH3:33])[C:5](=[O:31])[CH:6]=[C:7]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[N:20]=NC1C=C(C)C(O)=C(C)C=1)[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)([CH3:3])[CH3:2]>C(O)C>[CH:32]([N:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:31])[CH:6]=[C:7]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[NH2:20])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)([CH3:34])[CH3:33]

Participants

3

Reactant 1

HCID 136364246HCID 136364246, compound

Product 1

HCID 54145726HCID 54145726, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

N,N-Diisopropyl-3-[2-(3,5-dimethyl-4-hydroxyphenylazo)phenyl]-3-phenylpropenamide (2.58 g, 5.68 mmol) was treated as described in Example 28.3. The crude residue gave crystals from aqueous ethanol. Yield 1.23g (67%).

Sources & evidence

ORD record
ord-db8e511aa209414f82eb32a79fc93e6c
Source dataset
uspto-grants-2001_11
Patent number
US06313132B1

Reaction notes

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