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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 428456Generated: October 29, 2026

HCID 54378998, compound → HCID 54526015, compound

https://huagongshe.com/reaction/428456

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 54378998HCID 54378998—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 54526015HCID 5452601587.9%

Reaction Steps

340 mg of 6-benzyl-8-(methoxyimino)-2-methyl-2,6-diazaspiro[3,4]octane was dissolved in 10 ml of methanol and thereto 300 mg of 10% Pd-C was added. The resulting mixture was stirred for 2 hours at 50° C. under the pressure of hydrogen, filtered and concentrated under the reduced pressure to give 195 mg of the titled compound(yield: 85.2%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06313299B1
Source datasetuspto-grants-2001_11
ORD IDord-78dc34a6f6534a5a876f59018813fcdb
Source noteuspto-grants-2001_11