HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy](1,2-epoxy) styrol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]styrol | HCID 18359165 | — |
| Solvent | Cyclohexane ethylacetate | HCID 21867204 | — |
| Product | 2,3-Dichloro-4,5bis-[(2-methoxyethoxy)-methoxy](1,2-epoxy) styrol | HCID 18359067 | 99.6% |
Reaction Steps
Using the procedure of Stage D of Example 40, 13.2 g of thee allylic alcohol of Step C and 10.3 g of m-chloro perbenzoic acid were reacted to obtain 13.7 g of the expected product with a Rf=0.25 (AcOEt-cyclohexane 6-4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313305B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-27dfe7a18f6841e7807ea2c7744c6445 |
| Source note | uspto-grants-2001_11 |