HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → 2-Chloro-4,5-bis-[(2-methoxyethoxy)-methoxy]-styrol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | 2-Chloro-4,5-bis-[(2-methoxyethoxy)-methoxy]-styryl-carboxylate | HCID 73431877 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 2-Chloro-4,5-bis-[(2-methoxyethoxy)-methoxy]-styrol | HCID 18359182 | 34.2% |
Reaction Steps
Using the procedure of Stage C of Example 40, 60.8 g of the ester of Stage C and 293 ml of a molar solution of diisobutyl-aluminum hydride in hexane were reacted to obtain 18.5 g of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06313305B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-a4556e844f0b479d9d19fa9289fefd1c |
| Source note | uspto-grants-2001_11 |