HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 178418361, Verbindung → HCID 178453600, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Edukt | HCID 178453603 | HCID 178453603 | — |
| Katalysator | Platinum oxide (PtO) | HCID 82844 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | HCID 178453600 | HCID 178453600 | — |
Reaktionsschritte
trans-(4-Azidomethyl-cyclohexylmethyl)-carbamic acid tert-butyl ester (24 g) in ethyl acetate (1 liter) is hydrogenated over platinumoxide (2.4 g) at ambient temperature under atmospheric pressure of hydrogen. The catalyst is filtered-off and the filtrate concentrated to yield trans-(4-aminomethyl-cyclohexylmethyl)-carbamic acid tert-butyl ester as an oil. Rf(C2) 0.41.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06316203B1 |
| Quelldatensatz | uspto-grants-2001_11 |
| ORD ID | ord-9b5f6e004cea4a23a789423b98b3bc9e |
| Quellennotiz | uspto-grants-2001_11 |