HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 20703623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 18354407 | HCID 18354407 | — |
| Product | HCID 20703623 | HCID 20703623 | — |
Reaction Steps
The title compound was prepared from 2-[benzimidazol-1-yl]-4-[1-(1-(benzyloxycarbonyl)-4-(N-naphth-1-yl-carbamoyl)-piperazine-2-yl)ethylamino]pyrimidine (50 mg), 37% aqueous formaldehyde (17 μL), and NaBH3CN (4.4 mg) according to the procedure described in EXAMPLE 14, Step G. Mass spectrum (ESI) 507.4 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316444B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-8c76960d2f354e5a8c0a81cf4fe48589 |
| Source note | uspto-grants-2001_11 |