HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → HCID 70213506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | Sodium cyanoborohydride | HCID 5003444 | — |
| Reactant | HCID 20703610 | HCID 20703610 | — |
| Product | HCID 70213506 | HCID 70213506 | — |
Reaction Steps
The title compound was prepared from (S,S)-2-[1-(4-(N-naphth-1-yl-carbamoyl)-piperazin-2-yl)-ethylamino]-4-[benzimidazol-1-yl]pyrimidine (EXAMPLE 36, Step C; 12.5 mg), 4-pyridinecarboxaldehyde (16.4 mg), and sodium cyanoborohydride (3.1 mg) according to the procedure described in Example 14, Step G. Mass spectrum (ESI) 585.0 (M+2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316444B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-70b9b4d33fdd44e3830a4253e3965aad |
| Source note | uspto-grants-2001_11 |