HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 131721747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 131721748 | HCID 131721748 | — |
| Product | HCID 131721747 | HCID 131721747 | — |
Reaction Steps
From (+,−) cis 7-Benzyloxy-4-[4-(4-chlorobutyloxy)-phenyl]-3-phenyl-chroman (300 mg, 0.60 mmol) and morpholine (240 mg, 3 mmol). Reaction time 4 days. The evaporated product was crystallised from ether-petrolether, and further purified by silica column chromatography using methanol-methylene chloride (1+19) as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06316494B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-b97aa425a566460c8a0a6f99be0c1f6b |
| Source note | uspto-grants-2001_11 |