1-Bromohexane → HCID 18356289, compound

HRID 429505Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:7]=[C:8]([O:10][CH3:11])[CH:9]=1)[NH2:6].[CH2:12](Br)[CH2:13][CH2:14][CH2:15][CH2:16][CH3:17]>>[CH2:12]([N:6]([CH2:5][CH2:4][CH2:3][CH2:9][CH2:8][CH3:7])[C:5]1[CH:7]=[C:8]([O:10][CH3:11])[CH:9]=[C:3]([O:2][CH3:1])[CH:4]=1)[CH2:13][CH2:14][CH2:15][CH2:16][CH3:17]

Participants

Reactant 2

HCID 81011-Bromohexane

HCID 663013,5-Dimethoxyaniline

Product 1

HCID 18356289HCID 18356289, compound

Procedure

3,5-dimethoxyaniline was bromided with n-hexylbromide so as to obtain 1-di-n-hexylamino-3,5-dimethoxybenzene. This was nitrosoized so as to obtain 1-di-n-hexylamino-3,5-dimethoxy-4-nitrobenzene.

Sources & evidence

ORD record: ord-4b33f019b19a4a1ba26467d1ae298653
Source dataset: uspto-grants-2001_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06316605B1

Reaction notes

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