HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → 3-(3-Pentyl)benzyl bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | 3-(3-Pentyl)benzyl alcohol | HCID 54455151 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-(3-Pentyl)benzyl bromide | HCID 54104700 | 90% |
Reaction Steps
According to example 17, 1.84 g of 3-(3-pentyl)benzyl alcohol was treated with 0.34 mL of PBr3 in 25 miL of anhydrous CH2Cl2 to afford 2.23 g (90%) of 3-(3-Pentyl)benzyl bromide as a clear liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06319702B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-8b65a05ad6794824aa6651f2fd2c8de2 |
| Source note | uspto-grants-2001_11 |