Tetrafluoro-m-phenylenediamine dihydrochloride → 9,10-Anthracenedione, 1,4-bis((2-(dimethylamino)ethyl)amino)-5,8-dihydroxy-

HRID 430003Notes

Reaction equation

HRID 430003 reaction equation
C1(N)C(F)=C(F)C(F)=C(N)C=1F.Cl.Cl.[CH3:15][N+:16]([O-])([CH2:18][CH2:19][NH:20][C:21]1[CH:26]=[CH:25][C:24]([NH:27][CH2:28][CH2:29][N+:30]([O-])([CH3:32])[CH3:31])=[C:23]2[C:34]([C:36]3[C:41]([C:42](=[O:43])[C:22]=12)=[C:40]([OH:44])[CH:39]=[CH:38][C:37]=3[OH:45])=[O:35])[CH3:17]>>[CH3:31][N:30]([CH3:32])[CH2:29][CH2:28][NH:27][C:24]1[C:23]2[C:34](=[O:35])[C:36]3[C:41](=[C:40]([OH:44])[CH:39]=[CH:38][C:37]=3[OH:45])[C:42](=[O:43])[C:22]=2[C:21]([NH:20][CH2:19][CH2:18][N:16]([CH3:17])[CH3:15])=[CH:26][CH:25]=1

Participants

3

Reactant 2

HCID 149026Tetrafluoro-m-phenylenediamine dihydrochloride2×HCID 9955116Banoxantrone

Product 1

HCID 1354689,10-Anthracenedione, 1,4-bis((2-(dimethylamino)ethyl)amino)-5,8-dihydroxy-

Procedure

The solid dihydrochloride should be stored in a sealed container in a cold dark place (preferably a freezer). Before opening such containers they should be allowed to warm to room temperature, since the dihydrochloride (and AQ4N) absorb moisture particularly rapidly when cold.

Workup

  1. customabsorb moisture particularly rapidly when cold

Sources & evidence

ORD record
ord-48938090c62842d98ebb00d0f1203e2c
Source dataset
uspto-grants-2001_11
Patent number
US06320063B1

Reaction notes

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