HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15450534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15450533 | HCID 15450533 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15450534 | HCID 15450534 | — |
Reaction Steps
5-Acetoxybenzo[b]thiophene-3-carboxylic acid (12) (1,349 mg) prepared above was refluxed for 1.5 hours with dimethylformamide (1 drop), thionyl chloride (1.22 ml) and toluene (25 ml). The solvent was removed under reduced pressure to provide 1,454 mg of the title compound (13).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06320060B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-5aace94292c84aedab8856971f8942b7 |
| Source note | uspto-grants-2001_11 |