3,4-Dichlorobenzaldehyde → HCID 11182161, compound

Participants

Reaction Steps

Title compound was prepared by the procedure described in Example 61d, using sodium acetate (0.020 g, 0.242 mmol), sodium cyanoborohydride (0.012 g, 0.194 mmol), 3,4-dichlorobenzaldehyde (0.017 g, 0.0969 mmol), and 2-[((1R,2S)-2-aminocyclopentylmethyl)amino]-1H-quinolin-4-one dihydrochloride (0.032 g, 0.0969 mmol). δH (CD3OD) 1.25-2.05 (7H, m), 2.73-2.81 (1H, m), 3.10-3.29 (2H, m), 3.61-3.80 (2H, m), 5.56 (1H, s), 7.13-8.00 (7H, m,). MS (AP+) 416 (M+).

Provenance & Evidence