3-Methoxypropylamine → 2,2'-((3-Methoxypropyl)imino)bisethanol

HRID 430422Notes

Reaction equation

COCCCN.[CH2:7]1[O:9][CH2:8]1.C[O:11][CH2:12][CH2:13][N:14]([CH2:18][CH2:19]O)[CH2:15][CH2:16][OH:17]>>[CH3:7][O:9][CH2:8][CH2:19][CH2:18][N:14]([CH2:15][CH2:16][OH:17])[CH2:13][CH2:12][OH:11]

Participants

Reactant 3

HCID 16723-Methoxypropylamine

HCID 6354Ethylene Oxide

HCID 13635719Methoxyethyldiethanolamine

Product 1

HCID 126234322,2'-((3-Methoxypropyl)imino)bisethanol

Procedure

3-Methoxypropylamine (665.5 g, 7.466 mole) and ethylene oxide (624 g, 14.18 mole) were reacted as described above in the procedure for making methoxyethyldiethanolamine (Example 5 (i)). The material was analyzed and the neutralization equivalent was determined 177.13.

Sources & evidence

ORD record: ord-442bde9bcd4b4917aa868172910e74af
Source dataset: uspto-grants-2001_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06323167B1

Reaction notes

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