Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitrobenzaldehyde → 5-(4-Nitrophenyl)-1,3-dioxolo[4,5-g]-isochroman
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitrobenzaldehyde | HCID 541 | — |
| 반응물 | 2-(1,3-Dioxaindan-5-yl)ethan-1-ol | HCID 2759846 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 5-(4-Nitrophenyl)-1,3-dioxolo[4,5-g]-isochroman | HCID 404210 | 81% |
반응 단계
36.0 g (0.21 mol) of 2-(1,3-benzodioxol-5-yl)-ethanol is reacted with an equivalent amount of 4-nitrobenzaldehyde analogously to C.A. 105, 1986, 226357, and 50.7 g (81%) of the title compound, melting point 149-150° C. (ethanol), is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06323197B1 |
| 출처 데이터셋 | uspto-grants-2001_11 |
| ORD ID | ord-4240d1d38a9f4944846de6d24e713ac3 |
| 출처 메모 | uspto-grants-2001_11 |