HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-Enal → HCID 53741814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-Enal | HCID 307 | — |
| Reactant | Dipropylamine | HCID 8902 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 53741814 | HCID 53741814 | — |
Reaction Steps
Cinnamaldehyde (0.504 cm3, 4.0 mmol), di-propylamine (0.548 cm3, 4.0 mmol) and [Ir(COD)(dppb)][PF6] (0.070 g, 2 mol %) were treated as stated above, with 1,2-dichloroethane as solvent, and at approx. 1 bar H2 for 3 hours. The yield of product (N,N-di-n-propylcinnamylamine) obtained was 80.9%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06323370B1 |
| Source dataset | uspto-grants-2001_11 |
| ORD ID | ord-29b57b2af2a346cb981082282b3630e2 |
| Source note | uspto-grants-2001_11 |