HRID43096

反应详情

EQUATION

反应方程式

HRID 43096 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described in Step 14.1 but stirring the reaction mixture for 20 h at rt, using 6-(4-methylpiperazin-1-yl)-pyridin-3-ylamine (prepared as described in Example 33 but using N-methyl-piperazine in Step 33.2) and 8-(4-methyl-thiophen-3-yl)-quinoxaline-5-carboxylic acid (Example 67). Title compound: ESI-MS: 445.0 [M+H]+; tR=3.42 min (System 1).

WORKUP

后处理

  1. customThe title compound was prepared in analogy to the procedure