HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 430996Generated: October 30, 2026
Sodium Hydroxide → HCID 5297144, compound
https://huagongshe.com/reaction/430996
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,2-dimethyl-5,6-dinitrobenzimidazole | HCID 2729273 | — |
| Reactant | Tin atom | HCID 5352426 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 5297144 | HCID 5297144 | — |
Reaction Steps
1,2-Dimethyl-5,6-dinitrobenzimidazole was reduced with tin in hydrochloric acid. The solution obtained from the reduction was diluted with water, cooled to 10° C., and treated with 40% NaOH. The precipitate which formed was filtered, washed with water and recrystallized from alcohol to yield 1,2 dimethly-5,6 diaminobenzimidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06656940B2 |
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| Source dataset | uspto-grants-2003_12 |
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| ORD ID | ord-1852346d4b8545c09873d4a052afba8c |
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| Source note | uspto-grants-2003_12 |
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