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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 431146Generated: November 1, 2026

Benzyl mercaptan → HCID 11085502, compound

https://huagongshe.com/reaction/431146

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl mercaptanHCID 7509—
ReactantPhenylacetyleneHCID 10821—
ReactantSodiumHCID 5360545—
ProductHCID 11085502HCID 11085502—

Reaction Steps

A solution of phenylacetylene (0.02 mol) and benzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) was subjected to the Procedure 2, part A, to form (Z)-styryl benzylsulfide. The title compound was obtained in 65% yield by oxidation of the sulfide according to the Procedure 2, part B. 1HNMR (CDC13) δ4.50 (2H, s),6.65(1H, d, JH,H=11.2),7.18-7.74 (10H aromatic+1H ethylenic).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06656973B2
Source datasetuspto-grants-2003_12
ORD IDord-a7cf1e528d39492581657d48af82c21f
Source noteuspto-grants-2003_12