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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 431208Generated: October 31, 2026

Tert-Butyl isocyanide → HCID 22335578, compound

https://huagongshe.com/reaction/431208

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTert-Butyl isocyanideHCID 23577—
Reactant2,3-DichlorobenzaldehydeHCID 35745—
ReactantHCID 178418311HCID 178418311—
SolventPerchloric AcidHCID 24247—
ProductHCID 22335578HCID 22335578—

Reaction Steps

Compound 27 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 3-amino-1,2,4-triazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) tert-butylisonitrile solution (0.2 M, MC), 0.500 ml (0.15 mmol) 2,3-dichlorobenzaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%) in a substance library.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06657064B2
Source datasetuspto-grants-2003_12
ORD IDord-bd5137b3404945f2911ee119f9b0fc8e
Source noteuspto-grants-2003_12