HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 9796853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 2-Aminothiazole | HCID 2155 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Tert-Butyl isocyanide | HCID 23577 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 9796853 | HCID 9796853 | — |
Reaction Steps
Compound 40 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 2-amino thiazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) tert-butylisonitrile solution (0.2 M, MC), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%) and by reaction with acetyl chloride, the excess acetyl chloride being removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06657064B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-2b8e7534b892483abc65e080922baf49 |
| Source note | uspto-grants-2003_12 |