HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 508583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | HCID 508581 | HCID 508581 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 508583 | HCID 508583 | 21% |
Reaction Steps
A portion of the crude intermediate of example 58 above, (25 mg, 0.03 mmol) was added to a solution of ethanolamine in ethanol (1M, 10 mL). The resulting solution was stirred for 3 h before evaporation of the solvent. The residue was purified by preparative HPLC to yield 15 mg, 21% of the desired material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06656965B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-97450865205d462eb65ded66b272dfaa |
| Source note | uspto-grants-2003_12 |