HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15798843, compound → HCID 129677096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15798843 | HCID 15798843 | — |
| Reactant | HCID 21924245 | HCID 21924245 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 129677096 | HCID 129677096 | 73.4% |
Reaction Steps
To 1.00 g (4.63 mmol) of hydroxymethylferrocene of formula (30) below dissolved in 20 ml of methylene chloride was added dropwise 0.73 g (7.00 mmol) of chloride methacrylate in 5 ml of methylene chloride. The reaction solution was washed with an aqueous solution of NaCl, dilute hydrochloric acid and an aqueous solution of dilute sodium hydroxide and dried over sodium sulfate, followed by distillation of the solvent thereby obtaining 0.97 g (3.4 mmol) of ferrocenylmethyl methacrylate of formula (31):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06657768B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-e965427dbf9f41a6ba92a5bcd38cffa9 |
| Source note | uspto-grants-2003_12 |