HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 44303611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 69637249 | HCID 69637249 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 44303611 | HCID 44303611 | 103.1% |
Reaction Steps
0.27 g (0.43 mmol) of the compound obtained in step b) were dissolved in dichloromethane (1 ml). Trifluoroacetic acid (1 ml) was added and the reaction mixture was stirred for 2 h at room temperature. After evaporation of the solvents lyophilization gave the title compound (0.25 g, 86%) as a white amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06660728B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-be6044e598e04d5ba2fefead90b336ac |
| Source note | uspto-grants-2003_12 |