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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 431537Generated: October 31, 2026

Triethyl orthoacetate → HCID 22217732, compound

https://huagongshe.com/reaction/431537

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethyl orthoacetateHCID 66221—
ReactantHCID 22217957HCID 22217957—
ProductHCID 22217732HCID 22217732—

Reaction Conditions

Temperature100 °C

Reaction Steps

2-Amino-4-tert-butyl-6-nitrophenol was dissolved in triethyl orthoacetate (10 mL). The reaction mixture was stirred overnight at 100° C. Evaporation of volatiles in vacuo afforded 5-tert-butyl-2-methyl-7-nitrobenzoxazole (110 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06660732B2
Source datasetuspto-grants-2003_12
ORD IDord-52269a0be4d64ce9a856ae0453692233
Source noteuspto-grants-2003_12