1-(2-Methoxyphenyl)piperazine → HCID 9953209, compound

HRID 431639Notes

Reaction equation

HRID 431639 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]([CH3:25])[CH2:12][CH2:13]OS(C2C=CC(F)=CC=2)(=O)=O)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH3:26][O:27][C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][C:29]=1[N:34]1[CH2:39][CH2:38][NH:37][CH2:36][CH2:35]1>>[F:1][C:2]1[CH:3]=[CH:4][C:5]([S:8]([N:11]([CH2:12][CH2:13][N:37]2[CH2:36][CH2:35][N:34]([C:29]3[CH:30]=[CH:31][CH:32]=[CH:33][C:28]=3[O:27][CH3:26])[CH2:39][CH2:38]2)[CH3:25])(=[O:9])=[O:10])=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 13461-(2-Methoxyphenyl)piperazineHCID 54175908HCID 54175908, compound

Product 1

HCID 9953209HCID 9953209, compound

Procedure

The title compound was prepared using the procedure described in Example 1 using 4-fluorobenzenesulfonic acid 2-((4-fluorobenzenesulfonyl)-methyl-amino)-ethyl ester (D2) and 4-(2-methoxyphenyl)-piperazine. MH+ 408.

Sources & evidence

ORD record
ord-a94c26871e064a2f9dd4c41c12e65e19
Source dataset
uspto-grants-2003_12
Patent number
US06660751B1

Reaction notes

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