477327-26-7 → 477327-29-0

HRID 431818Notes

Reaction equation

HRID 431818 reaction equation
[C:1]1([C:7]2[CH:12]=[CH:11][C:10]([CH2:13][CH2:14]/[CH:15]=[CH:16]/[CH2:17][CH2:18][C:19]([O:21]CC)=[O:20])=[CH:9][CH:8]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>[OH-].[Na+]>[C:1]1([C:7]2[CH:12]=[CH:11][C:10]([CH2:13][CH2:14]/[CH:15]=[CH:16]/[CH2:17][CH2:18][C:19]([OH:21])=[O:20])=[CH:9][CH:8]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 1

HCID 59118337477327-26-7

Product 1

HCID 12097364477327-29-0

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

Ethyl E-7-((4-phenyl)phenyl)hept-4-enoate was saponified in methanolic sodium hydroxide at room temperature. The resulting acid, E-7-((4-phenyl)phenyl)hept-4-enoic acid, was obtained in >95% purity after chromatography. The product was fully characterized by spectral analysis infrared and nuclear magnetic spectroscopy) and combustion analysis.

Sources & evidence

ORD record
ord-afdd6d6dcb2d43258b4d299dbbddc76e
Source dataset
uspto-grants-2003_12
Patent number
US06660770B2

Reaction notes

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