HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenoxybenzoic acid → 3-Phenoxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenoxybenzoic acid | HCID 19539 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-Phenoxybenzoyl chloride | HCID 2760341 | — |
Reaction Steps
3-Phenoxybenzoic acid (214 mg, 1.0 mmol) was treated with a solution of oxalyl chloride (1.5 mL of 2 M in dichloromethane, 3 mmol) and a catalytic amount of N,N-dimethylformamide. The reaction was stirred overnight at ambient temperature. The excess oxalyl chloride was removed in vacuo to afford 3-phenoxybenzoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06660753B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-e763b04a7795469197e5ffe53186d938 |
| Source note | uspto-grants-2003_12 |