HRID432620

反应详情

EQUATION

反应方程式

HRID 432620 的结构方程式

PROCEDURE

实验过程

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (160 mg, 0.490 mmol) and phenol were reacted as starting materials at 120° C. for 22 hours and post-treatment was then conducted, whereby the title compound was obtained as colorless needles (133.1 mg, 70.7%). Melting point: 198.8-199.5° C. (ethyl acetate-hexane).

WORKUP

后处理

  1. customat 120° C.
  2. customfor 22 hours