HRID432621

反应详情

EQUATION

反应方程式

HRID 432621 的结构方程式

PROCEDURE

实验过程

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (352.5 mg, 1.08 mmol) and thiophenol were reacted as starting materials at 100° C. for 7 hours and post-treatment was then conducted, whereby the title compound was obtained as a colorless crystalline powder (55.8 mg, 12.9%). Melting point: 176.9-177.8° C. (chloroform-diethyl ether)

WORKUP

后处理

  1. customat 100° C.
  2. customfor 7 hours