HRID432624

反应详情

EQUATION

反应方程式

HRID 432624 的结构方程式

PROCEDURE

实验过程

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (200 mg, 0.613 mmol) and 2,5-difluorophenol were reacted as starting materials at 150° C. for 24 hours and post-treatment was then conducted, whereby the title compound was obtained as a colorless crystalline powder (235.5 mg, 91.5%). Melting point: 174.4-175.2° C. (chloroform-hexane).

WORKUP

后处理

  1. customat 150° C.
  2. customfor 24 hours