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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 432630Generated: October 31, 2026

2,4-Dichlorophenol → HCID 18760001, compound

https://huagongshe.com/reaction/432630

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,4-DichlorophenolHCID 8449—
Reactant3,4-Bis(4-methoxyphenyl)-6-chloropyridazineHCID 12568084—
ProductHCID 18760001HCID 18760001—

Reaction Steps

In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (150 mg, 0.495 mmol) and 2,4-dichlorophenol were reacted as starting materials at 150° C. for 15 hours and post-treatment was then conducted, whereby the title compound was obtained as a colorless crystalline powder (195.5 mg, 93.9%). Melting point: 152.2-152.8° C. (ethyl acetate-hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06664256B1
Source datasetuspto-grants-2003_12
ORD IDord-ccf18ec425404038b386e2be1e0210d1
Source noteuspto-grants-2003_12