HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenol → HCID 10295270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | 3,4-Bis(4-methoxyphenyl)-6-chloropyridazine | HCID 12568084 | — |
| Product | HCID 10295270 | HCID 10295270 | — |
Reaction Steps
In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (150 mg, 0.495 mmol) and 4-methoxyphenol were reacted as starting materials at 150° C. for 24 hours and post-treatment was then conducted, whereby the title compound was obtained as colorless prisms (180.1 mg, 94.7%). Melting point: 146.7-148.2° C. (ethyl acetate-diethyl ether-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-1d7c3a792cfe4a118c3228f44e41d742 |
| Source note | uspto-grants-2003_12 |