HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanophenol → HCID 18760039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | 3,4-Bis(4-methoxyphenyl)-6-chloropyridazine | HCID 12568084 | — |
| Product | HCID 18760039 | HCID 18760039 | — |
Reaction Steps
In a similar manner as in Example 2, 3,4-bis(4-methoxyphenyl)-6-chloropyridazine (150 mg, 0.459 mmol) and 4-cyanophenol were reacted as starting materials at 150° C. for 13 hours and post-treatment was then conducted, whereby the title compound was obtained as a pale yellow crystalline powder (108.0 mg, 57.5%). Melting point: 167.3-170.5° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664256B1 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-986cbdb6e47846e49f1f30db91870345 |
| Source note | uspto-grants-2003_12 |