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HRID43274

反应详情

EQUATION

反应方程式

HRID 43274 的结构方程式

REACTANTS

反应物

2
结构：CC(C)=O
HCID180

Acetone

C3H6O

结构：CC(C(=O)O)c1cc2c(s1)C=Cc1ccccc1C2=C1CCNCC1.O=S(=O)(O)c1ccccc1
HCID86665306

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)CCc1cc2c(s1)C=Cc1ccccc1C2=C1CCNCC1.O=S(=O)(O)c1ccccc1
HCID86665305

未命名化合物

收率 30%

PROCEDURE

实验过程

3-(4-Piperidin-4-ylidene-4H-1-thiabenzo[f]azulen-2-yl-propionic acid benzenesulfonate of 99.6% purity (1.0 g) was dissolved in acetone (50 mL) by heating and allowed to cool down to room temperature and the crystals deposited therefrom were filtered to give 0.30 g (recovery rate: 30%) of 3-(4-piperidin-4-ylidene-4H-1-thiabenzo[f]azulen-2-yl) propionic acid benzenesulfonate of 100% purity.

WORKUP

后处理

  1. temperatureby heating
  2. filtrationthe crystals deposited therefrom were filtered