HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → 1-tert-Butyl-3-ethyl-3,5,5-trimethylpiperazin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Methyl Ethyl Ketone | HCID 6569 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,2-Propanediamine, N1-(1,1-dimethylethyl)-2-methyl- | HCID 12580989 | — |
| Product | 1-tert-Butyl-3-ethyl-3,5,5-trimethylpiperazin-2-one | HCID 18760485 | 99% |
Reaction Steps
In analogy to Example B21, 1,1-dimethyl-2-t-butylaminoethylamin, methylethylketon, chloroform and NaOH are reacted to give the raw title compound (99%) as an yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06664353B2 |
| Source dataset | uspto-grants-2003_12 |
| ORD ID | ord-27d773ee409f497591cdd9b8d06e8646 |
| Source note | uspto-grants-2003_12 |